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Titrimetric Methods: Proceedings of the Symposium on Titrimetric Methods Held at
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Located in: Fairfield, Ohio, United States
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eBay item number:386714591181
Item specifics
- Condition
- Brand New: A new, unread, unused book in perfect condition with no missing or damaged pages. See all condition definitionsopens in a new window or tab
- ISBN-13
- 9781489927040
- Book Title
- Titrimetric Methods: Proceedings of the Symposium on Titrimetric
- ISBN
- 9781489927040
- Subject Area
- Science
- Publication Name
- Titrimetric Methods : Proceedings of the Symposium on Titrimetric Methods Held at Cornwall, Ontario, May 8-9 1961
- Item Length
- 9.3 in
- Publisher
- Springer
- Subject
- Chemistry / Physical & Theoretical, Chemistry / Analytic
- Publication Year
- 2013
- Type
- Textbook
- Format
- Trade Paperback
- Language
- English
- Item Height
- 0.2 in
- Item Width
- 6.1 in
- Item Weight
- 10.7 Oz
- Number of Pages
- VI, 185 Pages
About this product
Product Information
An analysis was needed which would indicate the purity and acid content of maleic anhydride. Small amounts of acid can affect the copolymerization behavior of the anhydride 1] and may cause rearrangement and polymerization of the diene component in Diels-Alder reactions 2]. Standardized solutions of tertiary amines such as tripropylamine and N-ethylpiperidine have been used by Siggia and Floramo 1] to titrate maleic and phthalic acids in their anhydrides. This method is rather specific for maleic acid since the acids which might be included in the determination are those with dissociation constants 3 of 10-, or greater, in water. This would not include 5 acids such as succinic (dissociation constant, 7 - 10- ) 4 or fumaric (9.3 - 10- ). Anhydrides have been determined in the presence of their acids by reaction with excess aniline and deter- mination of the excess 3]. The acid content is then found by difference in anhydride and total acidity by hydrolysis. Mixtures of anhydride and acid have been determined by difference using either sodium methylate in methanol to titrate the free acid plus one equivalent per mole of the anhydride and sodium hydroxide 4], or trimethyl- benzylammonium hydroxide 5] in the presence of water to titrate the free acid plus two equivalents per mole of the anhydride. The determination of free acid by the difference in the two titrations yields poor results for samples of low acid content.
Product Identifiers
Publisher
Springer
ISBN-10
1489927042
ISBN-13
9781489927040
eBay Product ID (ePID)
175686135
Product Key Features
Publication Name
Titrimetric Methods : Proceedings of the Symposium on Titrimetric Methods Held at Cornwall, Ontario, May 8-9 1961
Format
Trade Paperback
Language
English
Subject
Chemistry / Physical & Theoretical, Chemistry / Analytic
Publication Year
2013
Type
Textbook
Subject Area
Science
Number of Pages
VI, 185 Pages
Dimensions
Item Length
9.3 in
Item Height
0.2 in
Item Width
6.1 in
Item Weight
10.7 Oz
Additional Product Features
Number of Volumes
1 Vol.
Lc Classification Number
Qd450-882
Table of Content
Electrometric Titrations.- An Automatic Wet Chemical Analyzer for Process Monitoring and Control.- The Application of Coulometric Bromination Techniques to the Determination of Unsaturated Organic Compounds.- Combined Potentiometric Determinations of Manganese, Chromium, and Vanadium in Steels.- Complexometric Titrations.- The Use of Ethylenediamine Tartrate in Polarography.- A New Instrument for Automatic Colorimetric and Fluorimetric Titrations.- Titrations in Nonaqueous Solvents.- Nonaqueous Titrations (Keynote Address).- Complex Formation of Silver Ions with Phosphorus and Nitrogen Organic Compounds in Acetone Solutions.- Alkoxides of Quaternary Ammonium Bases. A New Type of Strongly Basic Titrants.- Application of Nonaqueous Titrimetry to Pharmaceutical Analysis.- A Rapid Determination of Maleic Acid and Maleic Anhydride in Mixtures of the Two.- Titrations of 1,4-Diphenylpiperazine.
Copyright Date
1961
Target Audience
Scholarly & Professional
Illustrated
Yes
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eBay item number:386714591181
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Fairfield, Ohio, United States
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Seller feedback (1,024,637)
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Book arrived safe and sound. Thanks!
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Novice users may wish to download and refer to Rodney J. Decker, An Introduction to the Bauer/Danker Greek-English Lexicon of the New Testament for an orientation and initiation on the use of the BDAG. The PDF comes up if you search "An Intro to using BDAG".
Grand Eagle Retail shipped this item in new condition, wrapped in plastic and shipped it safely and securely. Thanks Grand Eagle!.
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good deal. very timely delivery
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